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Chemische analyse van oestrogenen, organochloor en organostikstof pesticiden als mogelijke endocriene verstoorders in het Schelde-estuarium [Chemical analysis of estrogens, organochlorine and organonitrogen pesticides as possible endocrine disruptors Scheldt-estuary]
Citatie
Noppe, H.; De Brabander, H.; De Wasch, K.; Laboratory for Chemical Analysis - Ugent, Belgium; (2006): Chemical analysis of estrogens, organochlorine and organonitrogen pesticides as possible endocrine disruptors Scheldt-estuary.
Contact: Vakgroep Veterinaire Volksgezondheid & Voedselveiligheid (UGent-VVV), meer

Toegang tot data
Gearchiveerde data
Specifieke website

Gearchiveerd bestand:
Beschikbaarheid: Vrij beschikbaar na embargo periode
Data are initially restricted, but the access condition relaxes to academic or unrestricted once a specified period of time after an event (such as collection, publication, completion of QC procedures or project cessation) has elapsed

Beschrijving
Tussen 2002 en 2006 werden stalen genomen voor water, sediment, zwevende stof en biota langsheen de Westerschelde. Alle matrices werden geanalyseerd op oestrogenen, organochlorine en organostikstof pesticiden m.b.v. SPE, HPLC, GC-MS/MS en LC-MS/MS. meer

Met het oog op het inschatten van de potentiële risico's verbonden aan endocriene verstoorders, dient het voorkomen van deze stoffen te worden gedocumenteerd. Tussen 2002 en 2006 werden stalen genomen voor water, sediment, zwevende stof en biota langsheen de Westerschelde. Alle matrices werden geanalyseerd op oestrogenen, organochlorine en organonitrogeen pesticiden m.b.v. SPE, HPLC, GC-MS/MS en LC-MS/MS. Het doel van dit gedeelte van het ENDIS-RISKS project is het geven van een overzicht van het voorkomen en de concentraties van de geselecteerde endocriene verstoorders in het Schelde estuarium. Staalnames worden verricht met de Belgica R.V. drie maal per jaar.

Scope
Thema's:
Kustonderzoek (bv. stranden, estuaria), Milieu-kwaliteit / vervuiling
Kernwoorden:
Ecotoxicologie, Fungiciden, Herbiciden, Hormonen, Insekticiden, Oestrogenen, Pesticiden, Steroïden, Waterkwaliteit, ANE, Schelde-estuarium, ANE, Nederland, Westerschelde, Bath, ANE, Nederland, Westerschelde, Hansweert, ANE, Nederland, Westerschelde, Terneuzen, ANE, Nederland, Westerschelde, Verdronken Land van Saeftinge, ANE, Nederland, Westerschelde, Vlissingen, België, Zeeschelde, Antwerpen, België, Zeeschelde, Doel, Crangon crangon (Linnaeus, 1758), Neomysis integer (Leach, 1814)

Geografische spreiding
ANE, Schelde-estuarium [Marine Regions]
ANE, Nederland, Westerschelde, Bath Stations [Marine Regions]
S12
Coördinaten: Long: 4,225; Lat: 51,365 [WGS84]
ANE, Nederland, Westerschelde, Hansweert Stations [Marine Regions]
S07
Coördinaten: Long: 4; Lat: 51,4367 [WGS84]
ANE, Nederland, Westerschelde, Terneuzen Stations [Marine Regions]
S04
Coördinaten: Long: 3,825; Lat: 51,345 [WGS84]
ANE, Nederland, Westerschelde, Verdronken Land van Saeftinge Stations [Marine Regions]
S09
Coördinaten: Long: 4,0783; Lat: 51,37 [WGS84]
ANE, Nederland, Westerschelde, Vlissingen Stations [Marine Regions]
S01
Coördinaten: Long: 3,57; Lat: 51,4167 [WGS84]
België, Zeeschelde, Antwerpen Stations [Marine Regions]
S22
Coördinaten: Long: 4,3917; Lat: 51,2188 [WGS84]
België, Zeeschelde, Doel Stations [Marine Regions]
S15
Coördinaten: Long: 4,2733; Lat: 51,3133 [WGS84]

Spreiding in de tijd
2002 - 2006
Onbekend

Taxonomische spreiding
Crangon crangon (Linnaeus, 1758) [WoRMS]
Neomysis integer (Leach, 1814) [WoRMS]

Parameters
Alpha-Estradiol Methode , Atrazine Methode , Beta-Estradiol Methode , Chlordane, Endosulfan, Estrone Methode , Ethinylestradiol Methode , Kepone, Toxaphene, Vinclozolin
Alpha-Estradiol: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Alpha-Estradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Alpha-Estradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Alpha-Estradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS
Atrazine: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Atrazine: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Atrazine: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Atrazine: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS
Beta-Estradiol: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Beta-Estradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Beta-Estradiol: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Beta-Estradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS
Estrone: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Estrone: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Estrone: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Estrone: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS
Ethinylestradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Ethinylestradiol: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Ethinylestradiol: SPE GCMS/MS
(1) Description protocol for the detection of organonitrogen pesticides (atrazine, simazine, terbutylazine) in water samples: After pH adjustment, the samples are filtered and extracted using SDB solid phase extraction cartridges. The extracts are analysed by GC-MS/MS (EI). The data processing is performed by Xcalibur 1.3. and MSOffice Excel. The identification of the organonitrogen pesticides is based on the relative retention time and a specific mass spectrum. Quantification is performe

Ethinylestradiol: GC-EI-MS-MS
Description protocol for pesticides and estrogenes in biota, SPM and sediment: Extraction is performed using accelerated solvent extraction (ASE). After HPLC fractionation or clean-up using the SPE from water analysis samples are analysed bij GC-EI-MS-MS

Bijdrage door
Federaal Wetenschapsbeleid (BELSPO), meerdata eigenaar
Universiteit Gent; Faculteit Diergeneeskunde; Vakgroep Veterinaire Volksgezondheid & Voedselveiligheid (VVV), meer
Universiteit Gent; Faculteit Diergeneeskunde; Vakgroep Veterinaire Volksgezondheid & Voedselveiligheid; Laboratorium voor Chemische Analyse (LCA), meerdata eigenaardata creator

Gerelateerde datasets
Maakt deel uit van:
ENDIS-RISKS fysico-chemische data en hyperbenthos van de Schelde, 2002-2006., meer

Project
ENDIS-RISKS: Endocriene verstoring in het Schelde-estuarium: distributie, blootstelling en effecten, meer

Publicatie
Gebaseerd op deze dataset
Noppe, H. (2006). Analytiek van hormoon verstorende stoffen in milieumatrices = Analytics of endocrine disrupting chemicals in environmental matrices. PhD Thesis. Universiteit Gent. Faculteit Diergeneeskunde: Gent. ISBN 978-90-5864-100-7. 153 pp., meer
Noppe, H. et al. (2005). Development and validation of an analytical method for detection of estrogens in water. Anal. Bioanal. Chem. 382(1): 91-98. dx.doi.org/10.1007/s00216-005-3174-8, meer
Noppe, H. et al. (2006). Development and validation of an analytical method for detection of estrogens in water, in: Noppe, H. Analytiek van hormoon verstorende stoffen in milieumatrices = Analytics of endocrine disrupting chemicals in environmental matrices. pp. 21-41, meer
Noppe, H. et al. (2005). Endocriene verstoringen in het Schelde estuarium (1) = Endocrine disruptors in the Scheldt estuary (1), in: Mees, J. et al. (Ed.) (2005). VLIZ Young Scientists' Day, Brugge, Belgium 25 February 2005: book of abstracts. VLIZ Special Publication, 20: pp. 50, meer
Noppe, H. et al. (2007). Multi-analyte approach for the determination of ng.l-1 amounts of steroid hormones in unidentified aqueous samples. Anal. Chim. Acta 586(1-2): 22-29. https://dx.doi.org/10.1016/j.aca.2006.08.048, meer
Noppe, H. (2007). Occurrence of hormones in the Scheldt estuary: an analytical challenge!, in: Mees, J. et al. (Ed.) (2007). VLIZ Young Scientists' Day, Brugge, Belgium 2 March 2007: book of abstracts. VLIZ Special Publication, 39: pp. 14, meer

Dataset status: Afgelopen
Data type: Data
Data oorsprong: Onderzoek
Metadatarecord aangemaakt: 2004-05-10
Informatie laatst gewijzigd: 2017-11-17
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